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1 article(s) from Kuhwald, Conrad

Inductive heating and flow chemistry – a perfect synergy of emerging enabling technologies

Conrad Kuhwald,
Sibel Türkhan and
Andreas Kirschning

Beilstein J. Org. Chem. 2022, 18, 688–706, doi:10.3762/bjoc.18.70

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Graphical Abstract

Figure 1: Inductive heating, a powerful tool in industry and the Life Sciences.

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Figure 2: Electric displacement field of a ferromagnetic and superparamagnetic material.

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Figure 3: Temperature profiles of reactors heated conventionally and by RF heating (Figure 3 redrawn from [24]).

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Scheme 1: Continuous flow synthesis of isopulegol (2) from citronellal (1).

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Scheme 2: Dry (reaction 1) and steam (reaction 2) methane reforming.

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Scheme 3: Calcination and RF heating.

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Scheme 4: The continuously operated “Sabatier” process.

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Scheme 5: Biofuel production from biomass using inductive heating for pyrolysis.

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Scheme 6: Water electrolysis using an inductively heated electrolysis cell.

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Scheme 7: Dimroth rearrangement (reaction 1) and three-component reaction (reaction 2) to propargyl amines 8 ...

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Figure 4: A. Flow reactor filled with magnetic nanostructured particles (MagSilica^TM) and packed bed reactor ...

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Scheme 8: Claisen rearrangement in flow: A. comparison between conventional heating (external oil bath), micr...

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Scheme 9: Continuous flow reactions and comparison with batch reaction (oil bath). A. Pd-catalyzed transfer h...

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Scheme 10: Continuous flow reactions and comparison with batch reaction (oil bath). A. pericyclic reactions an...

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Scheme 11: Reactions under flow conditions using inductively heated fixed-bed materials serving as stoichiomet...

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Scheme 12: Reactions under flow conditions using inductively heated fixed-bed materials serving as catalysts: ...

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Scheme 13: Two step flow protocol for the preparation of 1,1'-diarylalkanes 77 from ketones and aldehydes 74, ...

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Scheme 14: O-Alkylation, the last step in the multistep flow synthesis of Iloperidone (80) accompanied with a ...

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Scheme 15: Continuous two-step flow process consisting of Grignard reaction followed by water elimination bein...

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Scheme 16: Inductively heated continuous flow protocol for the synthesis of Iso E Super (88) [91,92].

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Scheme 17: Three-step continuous flow synthesis of macrocycles 89 and 90 with musk-like olfactoric properties.

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Review

Published 20 Jun 2022

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